LITHIUM HEXAMETHYLDISILAZIDE, 0.85M in hexane (19-21 wt %)

Product Code: SIL6467.2
CAS No: 4039-32-1
SDS Sheets: EU | US
COMMERCIAL
4039-32-1
Pack Size
Quantity
Price
 
100 g
$80.00
2.5 kg
$447.50
12.5 kg
$1,162.50
135 kg
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Product data and descriptions listed are typical values, not intended to be used as specification.

  • HMIS

    3-4-1-X
  • Molecular Formula

    C6H18LiNSi2
  • Molecular Weight (g/mol)

    167.33
  • TSCA

    Yes
  • Boiling Point (˚C/mmHg)

    NA
  • Density (g/mL)

    0.716
  • Flash Point (˚C)

    -23 °C

Additional Properties

  • Hydrolytic Sensitivity

    7: reacts slowly with moisture/water
  • Application

    Review of synthetic utility.1
    Used in the use of chloroform in the trichloromethylation of a ketone in a scaled-up synthesis of ?-secretase inhibitor, spiropiperidine.2

    Reference

    1. Handbook of Reagents for Organic Synthesis, Reagents for Silicon-Mediated Organic Synthesis, Fuchs, P. L. Ed., John Wiley and Sons, Ltd., 2011, p. 356-367.
    2. Henegar, K. E. et al. Org. Process. Res. Dev. 2013, 17, 985.

    Safety

  • Packaging Under

    Nitrogen